NMR spectra are typically collected in solutions made up of deuterated solvents due to the fact that a protonated solvent will yield large solvent peaks which may hide the solute’s spectral features.
NMR spectroscopy is among the most powerful analytical techniques for the elucidation of chemical structure. It has the capability of providing detailed information about structure and dynamics of ...
AMES, Iowa – A tiny, solid sample of a drug, complete with active and inactive ingredients, spun at 50,000 revolutions per ...
This technique’s ability to highlight molecular structure and track reaction dynamics has garnered widespread recognition throughout academia and industry as a robust, nondestructive, noninvasive ...
This whitepaper explores the development and implementation of such procedures using the Bruker Fourier 80 benchtop NMR spectrometer. Through examples involving model drug products, it highlights how ...
If the sample does not lock, please make sure that you followed the "NMR-basic-operation" procedure, in particular, make sure that you followed the procedure about sample preparation. Do you have ...
New work from Georgia Tech is showing how a simple glass of wine can serve as a powerful gateway for understanding advanced ...
Unfortunately, many 1H-NMR spectra are severely overlapped due to the multiplet structure caused by homo-nuclear scalar couplings. "Pure shift" NMR spectra, also known as broadband homonuclear ...
For the majority of users conducting nuclear magnetic resonance (NMR) spectroscopy today, sample preparation follows a similar path: isolate a compound or compounds from a reaction mixture (or if ...
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